Synthesis, Characterization and Stabilization Analysis of Ferrofluid Based on Amazon Vegetable Copaifera O. L. Oil
DOI:
https://doi.org/10.31686/ijier.vol9.iss7.3235Keywords:
magnetite, copaiba oil, magnetic fluidAbstract
The Nanoscience and Nanobiotechnology develops several researches using nanostructures with magnetic properties. These nanostructures can have different physical properties depending on their composition and therefore can be used in various applications such as: drug markers and carriers, microelectronics, magnetic separations and environmental applications. Furthermore, the use of natural components in the synthesis of these nanostructures may come to complement these nanomaterials due to their underexplored properties and their renewable origin. This research will aim to carry out a pre-study to analyze the stability of magnetic fluids based on Fe3O4 nanoparticles functionalized with vegetable oil from the Copaifera SPP plant, known as Copaiba. Therefore, the Fe3O4 nanoparticles will be synthesized by the coprecipitation method by hydrolysis in an alkaline solution. Ferrofluid will be prepared by dispersing magnetic nanoparticles, at different concentrations, in the “in natura” oil. For the samples characterization measurements were taken of: UV-vis, FTIR, NIR spectrophotometry, XRD and Magnetic Susceptibility, the temporal analysis was recorded periodically, observing the possible stability of the samples. This work reports that the ferrofluid showed good stability and the magnetic properties associated with the nanoparticles the properties of the Amazon oil used.
References
V.F. Veiga Jr and A. C. Pinto, “. O GÊNERO Copaifera L.”, Química Nova, Rio de Janeiro, 2002, v.5, n.2, p. 273-286. https://doi.org/10.1590/S0100-40422002000200016 DOI: https://doi.org/10.1590/S0100-40422002000200016
K. Monroe, T. Kirk, V. Hull, E. Biswas, A. Murawski and R. L. Quirino, “Vegetable Oil-Based Polymeric Materials: Synthesis, Properties, and Applications.”, Elsevier Ltd., 2020, p. 1-8. https://doi.org/10.1039/c0gc00264j DOI: https://doi.org/10.1016/B978-0-12-803581-8.11521-8
X. Wang, C. Li, Y. Zhang, D. Wenfeng, M. Yang, T. Gao, H. Cao, X. Xu, D. Wang, Z. Said, S. Debnath, M. Jamil and H.M. Ali, “Vegetable oil-based nanofluid minimum quantity lubrication turning: Academic review and perspectives”. Journal of Manufacturing Processes, 2020, v. 59, n. September, p. 76–97. https://doi.org/10.1016/j.jmapro.2020.09.044 DOI: https://doi.org/10.1016/j.jmapro.2020.09.044
O. C. Rigamonte-Azevedo, P. G. Salvador Wadt, L. H. O. Wadt, “Potencial de produção de óleo-resina de copaíba (Copaifera spp) de populações naturais do sudoeste da Amazônia”, Revista Arvoré, 2006, v. 30, n. 4, p. 538-591. https://doi.org/10.1590/S0100-67622006000400011 DOI: https://doi.org/10.1590/S0100-67622006000400011
S. Laurent, D. Forge, M. Port, A. Roch, C. Robic, L. Vander Elst, R. N. Muller, “Magnetic iron oxide nanoparticles: synthesis, stabilization, vectorization, physicochemical characterizations, and biological applications”, Chemical reviews, 2008, v. 108, n. 6, p. 2064–110. https://doi.org/10.1021/cr068445e DOI: https://doi.org/10.1021/cr068445e
Y. S. Kang, S. Risbud, J.F. Rabolt, P. Stroeve, “Synthesis and characterization of nanometer-size Fe3O4 -Fe2O3 particles”, Chem. Mater., 1996, v. 8, p. 2209-2211. https://doi.org/10.1021/cm960157j DOI: https://doi.org/10.1021/cm960157j
W. Wu, Q. He, C. Jiang, “Magnetic iron oxide nanoparticles: synthesis and surface functionalization strategies”, Nanoscale research letters,2008, v. 3, n. 11, p. 397–415. https://doi.org/10.1007/s11671-008-9174-9 DOI: https://doi.org/10.1007/s11671-008-9174-9
L. G. F. Silva, H. P. Pacheco, J. G. Santos, and L. B. Silveira. “A Hybrid Nanocomposite from γ-Fe2O3 Nanoparticles Functionalized in the Amazon Oil Polymers Matrix”. International Journal for Innovation Education and Research 8, 2020, n. 6, p. 418–425. https://doi.org/10.31686/ijier.vol8.iss6.2435 DOI: https://doi.org/10.31686/ijier.vol8.iss6.2435
R. Tietze, S. Lyer, S. Dürr, T. Struffert, T. Engelhorn, M. Schwarz, E. Eckert, T. Göen, S. Vasylyev, W. Peukert, F. Wiekhorst, L. Trahms, A. Dörfler, C. Alexiou, “Efficient drug-delivery using magnetic nanoparticles--biodistribution and therapeutic effects in tumour bearing rabbits” Nanomedicine: nanotechnology, biology, and medicine, 2013, v. 9, n. 7, p. 961–71. https://doi.org/10.1016/j.nano.2013.05.001 DOI: https://doi.org/10.1016/j.nano.2013.05.001
J. Lee, T. Isobe, M. Senna, “Preparation of ultrafine Fe3O4 particles by precipitation in the presence of pva at high pH.” Journal of colloid and interface science, 1996, v. 177, p. 490-494. https://doi.org/10.1006/jcis.1996.0062 DOI: https://doi.org/10.1006/jcis.1996.0062
J. B. Mamani, A. J. Costa-Filho, D. R. Cornejo, E. D. Vieira, L. F. Gamarra, “Synthesis and characterization of magnetite nanoparticles coated with lauric acid”, Materials Characterization, 2013, v. 81, p. 28–36. https://doi.org/10.1016/j.matchar.2013.04.001 DOI: https://doi.org/10.1016/j.matchar.2013.04.001
A. Y. Takeuchi, Técnicas De Medidas Magnéticas, Livraria da Física, Brazil, 2010 pp. 80.
SILVERSTEIN, R. M., FRANCIS, X. W., D. J, Kernie and D. L. Bryce, Identificação Espectrométrica de Compostos Orgânicos, Editora LTC, 2019, p. 468.
F. S. Silva, L. G. F. Silva, P. I. Araújo Neto, A. B. Oliveira, “Estudo sobre a estabilidade de ferrofluídos
baseados em nanopartículas de Fe3O4 funcionalizadas em óleo vegetal”, Revista Amazontech, 2021, v.3, n.1, p. 62-70. https://revistaamazontech.com/
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Accepted 2021-06-29
Published 2021-07-01
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